Apr 8, 2018 · Vial Eq time: 45min Vial Pressurization time: 0.2min Injection time: 0.2min Loop fill time: 0.2min Loop Eq. Time: 0.2min GC Cycle time: 22min Shake: High Sample is 100mg of SSG in 20mL headspace vial. Add 5.0mL of DMSO. Please note that this has happened about a week ago.